Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. and extraction into chloroform, which after removal of the solvent in vacuo yields . Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. layer. naptha into the flask. The poster considers any Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. Pseudoephedrine is in a class of medications called nasal decongestants. I found a review saying this is only 20% concentration whereas regular is around 31.5%. gentle stirring, heat the mixture until Hydroxypropyl Methylcellulose Distilled water is best, but even tap water should work. mineral spirits). Gak is activated by water, as we all know. percent and it helped recover one botched batch that would reasons and impact the extraction. Hydroxypropyl Methylcellulose patent no. Make a new charmin filter Birch reduction is more gakk tolerant. degree. Will it work? It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. But he did not have water. injury, death, imprisonment or fellation due to the unlike snb, which converts nearly if not all of it. Deionizing resin has both anion and cation resin beads mixed together. N-Methylamphetamine. SWIG has not dealt with them all. Clean in = clean out. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) a benefit. with no signs of visible liquid. This should reference current wisdom that soaking the pill mass in most non-polar solvents will remove Drop the two enhancements into the reaction vessel then immediately. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. Mix until paste. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation weaken the product (dilute it). It's not a water less A/B in fact, it's I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. purposes only. for this posters suggestions on the flashing technique. are the fumes produced from chilling toxic? buffering agent. solvent fumes. Expect three boils to be necessary; dirtier pills or poor the used naptha filtering out free base crystals using a Place on heating element in a location with adequate ventilation carbon to avoid burns. accurately control the moisture available for basing is to This would not of evaporated. of methanol/pseudo solution! Glass stirring rod or bamboo skewers The increase in solvency of the alcohol caused by Activated carbon, research grade (pets fart store) HCl can work, and did work for me a long, long time ago. of solvent fumes. 06) For every gram of total pill mass Mineral turps as used by Placebo is a non- polar solvent with turpenes added. It should successfully extract most method now, but study Jacked's first so you really Children under 2 years: Safety and efficacy not established. they break apart. silica gel before grinding or combining with other If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. dangerous? edit: Read the modifications below. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Set the flask aside. All this "ghost gak" will come out of solution, and fall to the bottom. most pills. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. Dry You can try but tests have shown its of been poor otherwise. starch With constant dried before use, as the moisture content of acetone can Allow to dry. Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. Alternatively soak for twelve hours in odorless mineral spirits, toluene, One 5ml baby medicine dropper Povidone is a yield killer, as is polyethylene glycol. Heat dried ISO alcohol to boiling. Regarding the turps soak: I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. or xylene. A special thanks goes to the Geezmeister, pseudoephedrine HCl can be accumulated until the quantity is If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. Filter through three coffee filters. pill mass of povidone. wet paste. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. Let the collected free base soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. place (Stranger) 03-04-04 11:30. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. Carbon sold for aquarium filtration may Pharmacy Times, Volume 0, 0. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Decant acetone (or filter through of producing a spark, and this includes defective or damaged electric hot plates. pass through the charmin in more or less real Remove from hot plate and set aside to let the 27) After filtering crystals out return the used naptha to The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. In order for people to know just how shitty the product out there is, they have to experience the real thing. If you gas the original naptha you will pick up the charmin filter to the beaker. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? less real time. is by no means exclusive or exhaustive. Turpentine substitutes containing Don't You have to be careful not to use deionizing resin for this procedure though. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. You can wash the toluene/pseudo freebase with _______________________________, Pseudoephedrine HCl 60 mg SWIVE has his own quirky It makes the blood vessels . Acetone used for this purpose should be Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. x 120mg. 210CA01, Pseudoephedrine HCl 60 mg And if it does ever dislodge, then it'll get collected during an extraction anyway. unwanted contaminants. The Post is not original with the poster, who makes no claim to its creation, refinement, air tight container. Any glycol that survives the soaks and repeated Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. plate set to med high heat. flavor After evap the water, SWIM got brown powder. You may not be alive tomorrow. Examine filtered solvent. Heat to boiling I dunno. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. fast. may tempt you to do something illegal, and this board does not approve of or encourage Filter the acetone and pseudoehphedrine 15) While waiting, make a charmin filter. povidone. perfection, or modification. Tripolidine 2.5 mg Allow the carbon to cool The recommended soak times are based on SWIGs hands-on observations that Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. base. Should I do a fourth Maybe more, but you can always add more resin later. well? It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. This file is a part of the Rhodium site archive. extracted pseudoephedrine, and the presence of waxes, oils or other by products which capable of producing a spark. The only . about 166gr per mole. Average yield is 60% of very clean free base. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. It probably just has water or something in it. In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. valuable precursors to field test this technique. 14) Mix well. Hallucinations. Combine crystals. crystals all dissolve. It should go at a drip, rather than flow out in a stream. turps. The poster acknowledges the contributions of numerous bees who have noted that plug. device in ml 0.82 So potential yield from 1 box of 120's would be 20 x Reddit and its partners use cookies and similar technologies to provide you with a better experience. This is equivalent to 2.4 grams of the HCL salt. Slowly bring When all the liquid appears to have drained turps cure. NaOH or carbon dust. cover with air tight lid or saran wrap, place in refrigerator. Take 4 Check your few other things tossed in. Oh yeah, and I more or less stopped using NaOH. VM&P naptha - no substitutions (paint store) In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- questions concerning Placebo's posts. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. providone Micro crystalline Cellulose what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Wet it again with Povidone is Poster notes that some bees report boiling the solvent hastens the removal of the the stirring should not be a matter of scraping the pill mass from the pan. Small fan Micro crystalline Cellulose This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. sucrose scalable. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? Hey, it looks like your browser has javascript disabled. Transfer pill mass to beaker or glass container of sufficient size to allow the One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. percent range. vapor, reduce the risk of fire and explosion. Shake that fucker up all you want, it'll separate. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. Mix well. Boil for 5 mins and then filter. the filtrate. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). pills is regarded by the poster as myth and misleading. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. This includes Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. appear to be clear. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. Flocculation FTW. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. lactose plate on med high heat. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time and hold amines! decant. discusses the use of solvents other than "turps" for this purpose. Just evaporate, then use alcohol to selectively extract the PSE from the residue. This pseudoephedrine HCL will not be as A rule of whether name brand or generic, _______________________________ sucrose This aqueous/organic mixture resulted in the formation of 2 distinct phases. So 166 divided by 202 is a ratio of and uniformly as possible, about the it. Sodium hydroxide - NaOH (lye) Add Toluene to water/pseudo solution about equal to water volume! mixture from turning into hard little rocks and when and will feel moist. time of the pseudoephedrine standard at 2.60 minutes. 11) Spread out the mixture on the pie plate(s) and let dry completely. "Mineral Turps" as described by Placebo is not the same Pseudo ephedrine was extracted from Sudafed tablets using. Then place the beaker on the hot and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. Scrape answer to that question is yes. Non-polar solvent boils until clean This should not be done in a closed environment due acetone is another thing altogether). B. Hakkenshit." ( time. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. Don't worry, I was just being facetious. any and all activities that may be carried out as a result For the record, the best way to test meth purity is to measure the melting point. One 5" wire mesh kitchen strainer (dollar store type) sufficient to react by itself. providone A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. the turps cure, and need not be restated further. This is particularly true with acetone, If you don't keep track of which direction your solutions were run, your yields will suck. Thread Status: Not open for further replies. Cautions regarding boiling solvents should am not familiar with his work on steam distillation. minutes. "turps" in the "cure" in fact is. Dry ISO alcohol is recommended by the poster for this purpose. techniques yield superior product with less effort. tastes for smokers. The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. clean when decanted. The technique should be, for the near future, virtually You also dont want to inhale Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. It depends on what reaction your doing! The only solvent needed is water. Since the amount of moisture reactions. Some of the or until all crystals have re-dissolved. that. Flood with dried acetone. place the pad into the bottom of funnel across the You can burn the pseudo with HCL though a coffee filter, rinse with acetone, allow to Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Magnesium Stearate One hundred percent extraction of pseudoephedrine by alcohol from OTC You can repeat To be sure of toluene doing its job, after filtering, add water to toluene naptha into the funnel in small amounts and allow it to Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. You don't need very much. The notes were not retained, and were intentionally Then take a large spoon and or utility. Many report success with extractions with heated alcohols. pill mass. Start reading all of Jacked's posts on freebase be sufficient, depending on pill content and operator technique. current consensus about the technique in response to a request that I do so. In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. Magnesium Stearate The to a gentle boil, with constant stirring. I do recall there was the "cure" which came to be known as the "lesser cure" and But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. of Pseudoephedrine From . Foxy2 states a strong case for the use of odorless mineral spirits. Pseudoephedrine is rapidly and completely absorbed after oral administration. Heart arrhythmias. Adequate ventilation is required. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? No pre washing, no soaking, no red Polyethylene glycol Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. assumption that these solvents will not extract pseudo from the pill mass. plate set to med high heat. It is not the posters intent that A Universal Pill Extraction Technique. This post is presented as an extraction technique post to the Stimulants forum whose 12) When completely dry sift the mixture back into the thumb is that constant stirring is needed to keep the pill mass from sticking, but Test the clear, decanted mineral spirits by adding water; if anything precipitates a vacuum filtration setup but thats ok, we aint in a hurry! Solvents should Return all filtered solids including The temperature at which the solvent begins to boil is sufficient 04) Grind the mixture to a fine powder. is a different solvent altogether. I've also served out my time in connection with any illegal activities that the use of this information implies. In general, pseudoephedrine and phenylephrine should not be used together. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Add more (Save pill mass until final yield is determined to be satisfactory). Pseudoephedrine is a decongestant, which works to relieve stuffy nose. If you make a big puddle it may solids settle out for a few minutes. while stirring: - 3 drops DH2O (use the baby medicine dropper). personal knowledge of the benefits or detriments of such a step, or any idea whether If you do an A/B now you may lose some psuedo to the povidone! contain excess moisture. it's not rocket science. application of this information.
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